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Beilstein J. Org. Chem. 2010, 6, 756–765, doi:10.3762/bjoc.6.89
Graphical Abstract
Scheme 1: Synthesis of the nitroxide-terminated P2VP-macroinitiator.
Figure 1: Plots of ln(M0/Mt) and molecular weight distribution vs time of the homopolymerization of 2VP at ■ ...
Figure 2: Plots of number average molecular weight vs conversion for the homopolymerization of 2VP for ■ 90 °...
Figure 3: Plot of number average molecular weight vs conversion for the homopolymerization of 2VP at 110 °C w...
Figure 4: MALDI-TOF MS of P2VP obtained for polymerizations stopped after 2, 4, 6, and 8 h. The samples were ...
Scheme 2: Degradation of nitroxide-terminated P2VP-macroinitiator by laser light irradiation.
Figure 5: MALDI-TOF MS of P2VP obtained for polymerizations stopped after 2 h. The samples were prepared by t...
Scheme 3: Synthesis of the bi-responsive block copolymers.
Figure 6: SEC traces for P2VP-block-PNIPAAm (solid line) and P2VP macroinitiator (dashed line).
Figure 7: Demonstration of the solution behavior. Polymers from left to right: P2VP, PNIPAAm, P(2VP)85-block-...
Figure 8: Titration of P2VP105-block-PNIPAAm332 (1g/L) in 0.02 N HCl with 0.1 N NaOH at room temperature.
Figure 9: Hydrodynamic radius distribution of P(2VP)105-b-P(NIPAAm)332 at ○ pH 7, T = 20 °C and ● pH 2, T= 45...